Abstract

The title mol­ecule, C32H30F2N2, a product of the condensation reaction of butane-2,3-dione and 4-fluoro-2-(1-phenyl­eth­yl)aniline, is located about an inversion centre. In the asymmetric unit, the dihedral angle between the planes of the benzene and phenyl rings is 84.27 (5)°. Neither hydrogen bonding nor aromatic stacking is observed in the crystal structure.

Highlights

  • The title molecule, C32H30F2N2, a product of the condensation reaction of butane-2,3-dione and 4-fluoro-2-(1-phenylethyl)aniline, is located about an inversion centre

  • Neither hydrogen bonding nor aromatic stacking is observed in the crystal structure

  • Supporting information for this paper is available from the IUCr electronic archives (Reference: RK2419)

Read more

Summary

Bruker APEXII CCD diffractometer

Absorption correction: multi-scan (SADABS; Bruker, 2008) Tmin = 0.808, Tmax = 0.852. V = 1329.0 (3) A 3 Z=2 Cu K radiation = 0.64 mmÀ1 T = 295 K 0.35 Â 0.28 Â 0.26 mm 5982 measured reflections 2507 independent reflections 2132 reflections with I > 2(I) Rint = 0.019. 166 parameters H-atom parameters constrained Ámax = 0.18 e A À3 Ámin = À0.15 e A À3. The title molecule, C32H30F2N2, a product of the condensation reaction of butane-2,3-dione and 4-fluoro-2-(1-phenylethyl)aniline, is located about an inversion centre. The dihedral angle between the planes of the benzene and phenyl rings is 84.27 (5). Neither hydrogen bonding nor aromatic stacking is observed in the crystal structure

Related literature
Special details
Full Text
Paper version not known

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.