Abstract
Hexagonal hydrogen molybdenum bronze was obtained from alkali decamolybdate with tunnel structure by the reduction with nascent hydrogen. A maximum amount of inserted hydrogen was H/Mo=1.5. Hydrogen insertion accompanied the change in the amount of structural water and the removal of alkali ions. NMR spectrum proved the existence of several types of proton. We proposed the various models of proton clusters and the proton distribution of each model. We also discussed the effect of alkali ions in the tunnel-site by the results of the simulation of NMR spectrum.
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