Abstract
The 13C chemical shielding tensors in a single crystal of β-quinol clathrate with trapped methanol molecules have been obtained by high resolution double resonance. A single shielding tensor instead of three for the trapped methanol molecule results from time-averaging. It is axially symmetric about the crystallographic c-axis and the anisotropy is about 0.29 times as large as that of polycrystalline methanol. These results suggest a new type of motion of the trapped molecules.
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