Abstract
The reaction of syndiotactic poly (methacrylic acid) and formamide above 100C yields a syndiotactic copolymer of methacrylic acid and dimethacryloylimide. The 13C-NMR spectra of the copolymers show resolved α-CH3 and C=O resonances which are evaluated to yield the triad probabilities. The triad statistics prove a nearly random formation of the cyclic imide along the polymer chain.
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