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Abstract
AbstractAccurate chemical shifts are now accessible with high field NMR spectrometers. After the recall of the basic formulae, methods are proposed to measure chemical shifts with a high precision. Using two coaxial rotors at the magic angle, the necessary parameters used for correction are measured. The influence of different factors on the precision of the NMR measurements is discussed. Some proposals are given for MAS experiments used with solid‐state samples. © 2007 Wiley Periodicals, Inc. Concepts Magn Reson Part A 30A: 184–193, 2007.
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