Abstract

Three diverse middle distillate fuels from Mobile, Alabama, Jacksonville, Florida, and Kirachi, Pakistan were analyzed to quantify the organic nitrogen compound distribution in each. Organo-nitrogen compounds were isolated by a mild acid extraction followed by a silica-gel adsorption procedure. The extraction process yielded three extracts for each fuel: a basic nitrogen extract in methylene chloride, a nonbasic nitrogen extract in methylene chloride, and a nonbasic nitrogen extract in methanol. The major compounds in each extract were identified by gas chromatography/mass spectrometry (GC/MS).

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