Abstract
A series of five catalysts of NiO-Al2O3 of varying content (IA-VA) were prepared at pH ∼ 10 and dried at 80°C using neutral mesoporous alumina composed of μ-Al2O3 and poorly crystalline boehmite. Structural changes produced upon heat treatment up to 700° C were followed using XRD, TG and DTA techniques. The surface texture of the samples was investigated by nitrogen adsorption at 77 K. The effect of soaking period on the resulting preparation and on its thermally treated products was also investigated (III Aa).
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