Ni<SUB>3</SUB>Ge単結晶における降伏応力の温度および方位依存性

Abstract

An investigation of the mechanical behavior of Ni3Ge was made. Flow stress measurements were made on single crystals with several different orientations. Slip systems were determined by two-surface trace analysis, and dislocation arrangements due to deformation were observed by transmission electron microscopy. The yield stress, obtained over the temperature range −196 to 800°C, increases with increasing temperature in the temperature range where {111} slip operates (positive temperature dependence), but it decreases as {001} slip commences. Critical resolved shear stress for {111}〈101〉 slip is orientation-dependent in this temperature range. The positive temperature dependence is pronounced even below room temperature, and the yield stress nearly doubles as the temperature is raised from −196 to 27°C. Electron microscope observation on dislocation arrangements in the specimens deformed at −196 and 27°C has revealed that the mobility of screw dislocations decreases with increasing temperature. These observations indicate that the positive temperature dependence of the yield stress is controlled by the mobility of screw dislocations. This decrease of mobility leading to the positive temperature dependence of the yield stress can be explained by thermally activated cross slip of screw dislocations from the (111) plane to the (010) plane.