Abstract
AbstractThe compounds Zr9W4S, Zr9Mo4S, and Zr9W4S1−xNixO3 have been prepared by high temperature techniques. They belong to the general group of K phases. Single crystal x‐ray diffraction analysis of the mixed nickel/sulfide (Zr9.2W3.8S0.7Ni0.3O3.0, R = 2.6%) reveals nickel substitution for sulfur, and confirms oxygen occupancy of interstitial sites.
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