Abstract
The long-awaited volume on synthetic chemistry in the series Methods and Principles in Medicinal Chemistry is now available.[...]
Highlights
139 6. 2 Crystallization 141 6.2.1 Spontaneous Crystallization 141 6.2.2 Diastereomeric Crystallization 1416. 3 Kinetic Resolution 144 6. 4 Chromatographic Techniques 147 6.4.1 Gas Chromatography 147 6.4.2 High-Performance Liquid Chromatography 6.4.2.1 Indirect HPLC Enantioseparations 6.4.2.2 HPLC Enantioseparations using Chiral Additives to the Mobile Phase 6.4.2.3 Direct HPLC Enantioseparations 6.4.2.4 Preparative Resolution of Enantiomers in LC 6.4.2.4.1 Elution Batch Chromatography 6.4.2.4.2 Closed-Loop Recycling Chromatography 156 6.4.2.4.3 Simulated Moving Bed Chromatography 159 6.4.3 Supercritical (Subcritical) Fluid Chromatography 164 6.5 Electromigration Techniques 164 6.6 Racemization 6.7 Method Selection Strategy
computational methods play a major role in the discovery and development of new drugs
214 8 Selective Glycosidation Reactions and their Use in Medicinal Chemistry
Summary
139 6. 2 Crystallization 141 6.2.1 Spontaneous Crystallization 141 6.2.2 Diastereomeric Crystallization 1416. 3 Kinetic Resolution 144 6. 4 Chromatographic Techniques 147 6.4.1 Gas Chromatography 147 6.4.2 High-Performance Liquid Chromatography 6.4.2.1 Indirect HPLC Enantioseparations 6.4.2.2 HPLC Enantioseparations using Chiral Additives to the Mobile Phase 6.4.2.3 Direct HPLC Enantioseparations 6.4.2.4 Preparative Resolution of Enantiomers in LC 6.4.2.4.1 Elution Batch Chromatography 6.4.2.4.2 Closed-Loop Recycling Chromatography 156 6.4.2.4.3 Simulated Moving Bed Chromatography 159 6.4.3 Supercritical (Subcritical) Fluid Chromatography 164 6.5 Electromigration Techniques 164 6.6 Racemization 6.7 Method Selection Strategy.
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