Abstract
A simple, highly efficient synthesis of A/B aromatic 16-oxasteroids by either an intra- or inter-molecular Diels–Alder reaction of 1,2-naphthoquinone dimethides, generated by the thermolysis of methyl cyclobuta [a] naphthalene- 2-carboxylate or cyclobuta [a]naphthalen-2-ylmethanol, is described.
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