Abstract
Mn-silicalite-1 (Mn 5.2Si 90.8O 192) was synthesized from Mn 2+ ion-exchanged magadiite. The characteristics of Mn-silicalite-1 were investigated using electron spin resonance, synchrotron X-ray powder diffraction, IR spectroscopy and chemical analysis. The measurements indicate that Mn 2+ ions replace Si in the silicalite-1 framework. The orthorhombic framework structure of calcined Mn-silicalite-1 has been determined. The space group is Pnma, with a=20.1017(3) Å, b=19.8826(4) Å, c=13.3758(3) Å.
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