Abstract
Cleavage of triple-decker compounds with cyclopentadienide leads to anionic mononuclear complexes, which react to form trinuclear complexes. Thus the hitherto relatively inaccessible compound [(1)·Co·(1)·Fe·(1)·Co·(1)] has been obtained in 29% yield from [(1)·Co·(1)·Co·(1)] via [(1)·Co·(1)]⊖. X-ray structure analysis confirmed the proposed tetra-decker geometry.
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