Abstract
Ammonium- and phosphoniumperfluorocyclobutane ylides ( 7–11), easily prepared from perfluorocyclobutene ( 1) and tertiary amines ( 2–4) or phosphines ( 5,6), smoothly react with primary or secondary alcohols ( 12–18) and carboxylic acids ( 19,20) with formation of alkyl fluorides ( 21–26) or acyl fluorides ( 27,28), respectively. A mechanism for the reaction is proposed.
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