New method for extracting fracture toughness of ceramic materials by instrumented indentation test with Berkovich indenter

Abstract

Applying finite element analysis, a method is proposed for evaluating fracture toughness of ceramic materials by instrumented indentation with Berkovich indenter. The crack-tip KI (Stress intensity factor) of Berkovich-produced crack is numerically calculated by using virtual crack closure technique, in particular, three kinds of crack pattern, i.e., radial crack, transition crack and half-penny crack are identified and their crack fronts meet the equi-KI requirement. The validity of the proposed method is verified by instrumented indentation tests on standard SRM2100 (Si3N4) and CRM156 (Fused Silica) samples. Comparison with six representative conventional indentation methods indicates that the proposed method has advantages including wide application range, high accuracy and applicability to different crack patterns. Additionally, it’s revealed that the conventional indentation fracture toughness formulae derived from Lawn-Evans-Marshall formula tend to exhibit larger test error when applied to materials of relatively high indentation work ratio We/Wt.