Abstract
Iminophosphoranes 3, obtained from the Baylis–Hillman adducts, reacted with 2-azidobenzoyl chloride to give the azides 4. The sequential reaction of azides 4 with triphenylphosphine and isocyanate produced 1H-pyrimido[2,1-b]quinazoline-2,6-diones 9 in the presence of sodium ethoxide via a tandem aza-Wittig/nucleophilic addition/intramolecular cyclization/isomerization reaction.
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