New aspects on the superplasticity of fine-grained 7475 aluminum alloys

Abstract

Thermomechanical processes were developed which give fine grain sizes of 6 and 8 μm in the 7475 Al alloy. Superplastic properties of this material were evaluated in the temperature range of 400 °C to 545 °C over the strain-rate range of 2.8 x 10-4 to 2.8 X 10-2 s-1. The maximum ductility exhibited by the alloy was approximately 2000 pct, and optimum superplasticity was achieved at a strain rate of 2.8 X 10-3 s-1 which is higher by an order of magnitude than other 7475 Al alloys. This result is attributed to the presence of fine dispersoids which maintain the fine grain size at high homologous temperatures. The flow stress and strain-rate sensitivity strongly depend on the grain size. The superplastic 7475 Al alloy has strain-rate sensitivities of 0.67 (6 μm) and 0.5 (13 μm) and an activation energy which is similar to the one for grain boundary diffusion of aluminum. Microstructural investigation after superplastic tests revealed zones free of dispersoid particles at grain boundaries primarily normal to the tensile direction. These dispersoidfree zones (DFZs) appear even after 100 pct elongation and are occasionally as large as 5 μm across. This result demonstrates the importance of diffusional flow in superplastic deformation of the fine-grained 7475 Al alloy especially at low elongations.