Abstract
An anaerobic thin-layer spectroelectrochemical cell design and fabrication is described. The cell's anaerobicity and spectroelectrochemical responce is demonstrated using methyl viologen dye and flavodoxin. A comparison between the new cell and bulk spectrocoulometric cells provides the following attractive features: (1) results for spectroelectrochemical characterization of methyl viologen agree very well; (2) no mediator dye is needed for the reduction of flavodoxin; (3) the time of analysis is considerably shortened (12 min compared to 12 h).
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