Abstract

A high-resolution neutron diffraction investigation of a nickel powder sample at room temperature was performed at three different experimental geometries using the ASTACUS diffractometer at Otaniemi. In spite of the correlation between adjacent channels, the diffraction patterns were analysed by the ordinary profile-refinement procedure adapted especially to the present conditions. The correctness of the results was supported by an analysis of the integrated intensities. The weighted mean value for the Debye-Waller parameter, BNi, of 0.425 (±0.065) Å2 was in reasonable agreement with literature values.

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