Abstract
Slurries of silicate rocks and their glasses and suspensions of clay minerals were introduced into an inductively coupled plasma with high-solids nebulizers. Grinding time and the associated particle size appeared to control the reliability of analytical calibration functions, and only for the very fine-grained clay mineral fractions (0.5–2 μm) could reliable calibrations be obtained. Ratioing of analyte signals to Sc II 361.384 nm from scandium present in the aqueous phase compensated for variations in nebulization.
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