Abstract
Rhodium(III)-catalyzed C–H activation has been promoted impressively with ligand-attached nanosheets of layered double hydroxides (LDHs), a natural and/or synthetic anionic layered compound. A yield of >99% and a regioisomeric ratio of >20:1 have been produced in the coupling of alkenes with N-(pivaloyloxy)benzamide. The nanosheets have been revealed to enhance the catalytic activity by affording the desired basicity and improve the regioselectivity by serving as the rigid substitution of α-amino acid ligands.
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