Abstract
Nanoparticles of a new Hg(II) one-dimensional coordination polymer, {[Hg(4-bpdb)I2] n , 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene} were synthesized by reaction of HgI2 and 4-bpdb by a sonochemical method. The new nanoparticles were characterized by scanning electron microscopy, X-ray powder diffraction (XRD) and FT-IR spectroscopy; [Hg(4-bpdb)I2] n was structurally characterized by single crystal X-ray diffraction. This compound consists of one-dimensional polymeric units of [Hg(4-bpdb)I2]. The thermal stability of [Hg(4-bpdb)I2] n was studied by thermal gravimetric (TG) and differential thermal analyses (DTA).
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