Abstract
Abstract The colourless com pound NaLiS has been prepared and its structure determined by single crystal X-ray diffraction techniques. The very hygroscopic NaLiS crystallizes in the tetragonal space group P4/nmm (Z = 2) with the cell parameters a = 402.6(1), c = 649.5(2) pm. The structure was solved from 720 counter reflections (216 symmetry independent reflections) by differential Fourier syntheses. Refining gives a least squares residue of 0.024. The anti-PbFCl-type structure is characterized by layers of LiS4/4-tetrahedra connected by their edges in two dimensions and 2 interspersed layers of sodium
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