Abstract
In the title compound, C14H10BrN3O4·CH4O, the dihedral angle between the two benzene rings in the hydrazone molecule is 5.8 (3)° and an intramolecular O—H⋯N hydrogen bond generates an S(6) ring motif. An O—H⋯O hydrogen bond occurs between the hydrazone molecule and the methanol solvent molecule. In the crystal, the components are linked by intermolecular N—H⋯O hydrogen bonds, forming chains along the a axis.
Highlights
In the title compound, C14H10BrN3O4CH4O, the dihedral angle between the two benzene rings in the hydrazone molecule is 5.8 (3) and an intramolecular O—H N hydrogen bond generates an S(6) ring motif
H atoms treated by a mixture of independent and constrained refinement max = 0.56 e Å3
The components are linked by intermolecular N—H O hydrogen bonds, forming chains along the a axis
Summary
C14H10BrN3O4CH4O, the dihedral angle between the two benzene rings in the hydrazone molecule is 5.8 (3) and an intramolecular O—H N hydrogen bond generates an S(6) ring motif. Absorption correction: multi-scan (SADABS; Sheldrick, 1996) H atoms treated by a mixture of independent and constrained refinement max = 0.56 e Å3 C14H10BrN3O4CH4O, the dihedral angle between the two benzene rings in the hydrazone molecule is 5.8 (3) and an intramolecular O—H N Hydrogen bond generates an S(6) ring motif.
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