Abstract
In the title compound, C16H15BrN2O5·2H2O, the dihedral angle between the two aromatic rings is 2.9 (2)° and an intramolecular O—H⋯N hydrogen bond is observed. One of the water molecule is disordered over two positions, with occupancies of 0.83 (3) and 0.17 (3). In the crystal structure, molecules are linked into a three-dimensional network by intermolecular O—H⋯O, O—H⋯(O,O), O—H⋯N and N—H⋯O hydrogen bonds. π–π interactions involving Br-substituted benzene rings, with a centroid–centroid distance of 3.552 (3) Å are also observed.
Highlights
In the title compound, C16H15BrN2O52H2O, the dihedral angle between the two aromatic rings is 2.9 (2) and an intramolecular O—H N hydrogen bond is observed
H atoms treated by a mixture of independent and constrained refinement max = 0.32 e Å3
One of the water molecule is disordered over two positions, with occupancies of 0.83 (3) and 0.17 (3)
Summary
Jiu-Fu Lu,a* Suo-Tian Min,a Hong-Guang Ge,a Xiao-Hui Jia and Yue-Fei Baib a School of Chemistry and Environmental Science, Shaanxi University of Technology, Hanzhong 723000, People’s Republic of China, and bThe School of Pharmaceutical
Sign-in/Register to view highlights & summary Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callMore From: Acta Crystallographica Section E Structure Reports Online
Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
