Abstract
The title compound, C15H14N2O2, is the product of the reaction of 2-hydroxybenzaldehyde and 3-methylbenzohydrazide. The dihedral angle between the substituted benzene rings is 19.5 (3)° and an intramolecular O—H⋯N hydrogen bond generates an S(6) ring motif. In the crystal, molecules are linked by N—H⋯O hydrogen bonds to generate C(4) chains propagating in [001] and C—H⋯O interactions to the same O-atom acceptor reinforce the chains.
Highlights
The title compound, C15H14N2O2, is the product of the reaction of 2-hydroxybenzaldehyde and 3-methylbenzohydrazide
H atoms treated by a mixture of independent and constrained refinement max = 0.59 e Å3
The title compound was synthesized by the reaction of 2-hydroxybenzaldehyde (1 mmol, 0.12 g) with 4-methylbenzohydrazide (1 mmol, 0.15 g) in absolute methanol (30 ml) at ambient condition
Summary
H atoms treated by a mixture of independent and constrained refinement max = 0.59 e Å3. R factor = 0.062; wR factor = 0.186; data-to-parameter ratio = 15.2. The title compound, C15H14N2O2, is the product of the reaction of 2-hydroxybenzaldehyde and 3-methylbenzohydrazide. The dihedral angle between the substituted benzene rings is 19.5 (3) and an intramolecular O—H N hydrogen bond generates an S(6) ring motif. Molecules are linked by N—H O hydrogen bonds to generate C(4) chains propagating in [001] and C—H O interactions to the same O-atom acceptor reinforce the chains
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More From: Acta Crystallographica Section E Structure Reports Online
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