Abstract
There are two molecules in the asymmetric unit of the title compound, C4H13NO2SSi. In the crystal, molecules are linked via intermolecular N—H⋯O hydrogen bonds, forming chains along [001]. The crystal studied was an inversion twin, the refined ratio of twin domains being 0.61 (9):0.39 (9).
Highlights
There are two molecules in the asymmetric unit of the title compound, C4H13NO2SSi
Molecules are linked via intermolecular N—HÁ Á ÁO hydrogen bonds, forming chains along [001]
H atoms treated by a mixture of independent and constrained refinement
Summary
Key indicators: single-crystal X-ray study; T = 150 K; mean (Si–C) = 0.003 A; R factor = 0.039; wR factor = 0.094; data-to-parameter ratio = 28.8. There are two molecules in the asymmetric unit of the title compound, C4H13NO2SSi. In the crystal, molecules are linked via intermolecular N—HÁ Á ÁO hydrogen bonds, forming chains along [001]. The crystal studied was an inversion twin, the refined ratio of twin domains being 0.61 (9):0.39 (9). Related literature For the original synthesis of the title compound, see: Roy (1993). For the synthetic application of the title compound, see: Roy et al (1993). See: Ni et al (1995); Chunechom et al (1998)
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