Abstract
Katritzky's well-established chemistry of benzotriazole [1] was applied to the synthesis of 1,2,3,4- tetrahydro-b-carboline, which have been traditionally prepared by Pictet-Spengler condensation2, Fischer cyclisation and other methods3.[...]
Highlights
Katritzky's well-established chemistry of benzotriazole [1] was applied to the synthesis of 1,2,3,4tetrahydro-b-carboline, which have been traditionally prepared by Pictet-Spengler condensation2, Fischer cyclisation and other methods3
For C18H17N5 (303.36): C 71.27, H 5.65, 23.09; Found: C 70.99, H 5.64; N, 22.83
Summary
Katritzky's well-established chemistry of benzotriazole [1] was applied to the synthesis of 1,2,3,4tetrahydro-b-carboline, which have been traditionally prepared by Pictet-Spengler condensation2, Fischer cyclisation and other methods3. This facile reaction of 1-hydroxymethylbenzotriazole 1 with tryptamine 2 yielded very high quantities of crystalline N-benzotriazol-1-yl-methyl-1,2,3,4-tetrahydro-b-carboline 3.
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