Abstract
The title compound, C9H9N3O6, was synthesized by the condensation of methyl 3,5-dinitrobenzoate and 2-aminoethanol. The non-centrosymmetric space group results in the formation of pseudo-chiral helices in the crystal structure, which exhibits a layer packing structure involving intramolecular N—H⋯O and O—H⋯O interactions.
Highlights
The title compound, C9H9N3O6, was synthesized by the condensation of methyl 3,5-dinitrobenzoate and 2-aminoethanol
Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: LX2057)
R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger
Summary
Key indicators: single-crystal X-ray study; T = 294 K; mean (C–C) = 0.004 A; R factor = 0.035; wR factor = 0.092; data-to-parameter ratio = 6.8. The title compound, C9H9N3O6, was synthesized by the condensation of methyl 3,5-dinitrobenzoate and 2-aminoethanol. The non-centrosymmetric space group results in the formation of pseudo-chiral helices in the crystal structure, which exhibits a layer packing structure involving intramolecular N—HÁ Á ÁO and O—HÁ Á ÁO interactions. Related literature For related literature, see: Lin & Smith (1981); Morehouse & McGuire (1959); Percec (1981, 1982); Walde (1962)
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