Abstract

ABSTRACTIn this study, multiwalled boron nitride microtubes (BNMTs) were synthesised from amorphous boron powder in pure nitrogen atmosphere controlled graphite furnace at 1300°C for 6 h with amorphous boron/manganese (IV) oxide (MnO2) catalyst mass ratio of 1/1. It was found that the synthesised BNMTs outer diameters and the lengths vary between 0.68 and 1.57 µm and between 6.79 and 31.23 µm, respectively, by the scanning electron microscope analysis. The surface layer of AISI 1040 steel material was coated with multiwalled BNMTs at 950°C for 4 h in a foundry furnace. Transport phenomena of BNMT molecules on surfaces of the steel were considered by diffusion. Neutrons from obtained 241Am-Be source were irradiated on the 58Fe nuclei. The irradiation properties of the without and with BNMT coated steel materials were studied in the field of gamma emitted by 60Co. The radiation exposure rate of gamma radiation sources used at 1099 and 1291 keV, respectively. The higher peak area was obtained in steel coated with BNMT according to non-coated steel from irradiation results of samples. These results show that BNMT coated steel was more capable for radiation shielding.

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