Multi-scale experimental deformation and damage initiation of clay-rich rocks  : Coupling ultrasonic wave propagation and  full field deformation measurements by digital image correlation (DIC)

Abstract

Understanding the damage processes in clay-bearing rocks is a decisive factor in geological engineering, and for instance considering nuclear waste deep geological repositories. But, more generally they may also contribute to localized deformation, and thus the rupture of fault gauges in seismic zones. However, owing to their complex mineralogy, multiscale microstructures and anisotropy, the mechanisms of clay-rich rock damage and their chronology are not yet well understood.. Here we focus on the impact of micro-damage on ultrasonic wave propagation velocity, which is confronted with the corresponding full deformation fields calculated by digital image correlation (DIC).  The aim is to associate the acoustic signature with the active deformation mechanisms identified by DIC. To this end, an integrated experimental approach is proposed to  characterize localization and to identify the related deformation micro-mechanisms  during uniaxial compression of natural clayey rock samples (Tournemire shales) with two simultaneous measurements: 1) the evolution of P-wave velocity within the sample by active acoustics, 2) the development of the 2D mechanical full field by digital image correlation. Both experimental techniques are well known, but the innovation of our approach is to combine simultaneously both measurements. Deformation localization is a multiscale problem, which obviously occurs at the sample scale, but also at the fines scales of the microstructure. Therefore, we developed two different experimental setups. On the one hand, during uniaxial compression with a standard MTS loading frame the macro-scale localization patterns are characterized by optical observations, which image resolution is well suited to the cm sample scale (sample diameter: 3.6 cm and double in length). On the other hand, in order to characterize the initiation of micro-damage at the microstructure scale of the composite type of rock, the same loading protocol is reproduced (while keeping the acoustic diagnosis) on smaller scale mm-sized specimens (sample diameter : 8 mm, double in length), using a home-designed miniature loading frame fit for an environmental scanning electron microscope (ESEM). The latter analysis is carried out under  controlled relative humidity  of RH = 80%, hence preventing the samples to dry out due to the high vacuum A similar acoustic signature is identified at both scales of observation, in spite of the variations of experimental conditions imposed by the environmental SEM. We are therefore confident to be able to understand the fracturing process from micro-cracking initiation (microscale) to sample failure (macroscale), and to assess its impact on ultrasonic wave propagation.