Abstract
A method that allows the extraction and simultaneous detection of organophosphate pesticides (OPs) and their primary and secondary metabolites from beef tissue was developed. High-performance liquid chromatography (HPLC) with UV-visible diode array detection was used. The OPs and metabolites were extracted from 10-g samples of lean (4.1% fat) and fatty (29.3% fat) beef muscle tissue. Recovery studies were performed at 1 ppm fortification levels in each sample type. Recoveries ranged from 45 to 95% in the lean muscle tissue
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