Abstract

X-ray microscopy is a successful technique with applications in several key fields. Fresnel zone plates (FZPs) have been the optical elements driving its success, especially in the soft X-ray range. However, focusing of hard X-rays via FZPs remains a challenge. It is demonstrated here, that two multilayer type FZPs, delivered from the same multilayer deposit, focus both hard and soft X-rays with high fidelity. The results prove that these lenses can achieve at least 21 nm half-pitch resolution at 1.2 keV demonstrated by direct imaging, and sub-30 nm FWHM (full-pitch) resolution at 7.9 keV, deduced from autocorrelation analysis. Reported FZPs had more than 10% diffraction efficiency near 1.5 keV.

Highlights

  • X-ray microscopy brings new insights to materials researchers from different fields by adding either a 3rd spatial [1,2] or a temporal [3,4] dimension to materials analysis, both at very high resolution

  • The results prove that these lenses can achieve at least 21 nm half-pitch resolution at 1.2 keV demonstrated by direct imaging, and sub-30 nm full width at half maximum (FWHM) resolution at 7.9 keV, deduced from autocorrelation analysis

  • The fabrication process is intrinsically capable of delivering Fresnel zone plates (FZPs) with high efficiency imaging performance at both soft and hard X-rays

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Summary

Introduction

X-ray microscopy brings new insights to materials researchers from different fields by adding either a 3rd spatial [1,2] or a temporal [3,4] dimension to materials analysis, both at very high resolution. The width of the outermost zone, Δr, defines its full-pitch resolution at 1st diffraction order, δRayleigh = 1.22Δr according to the Rayleigh criterion [10] Another important property of FZPs is their diffraction efficiency, DE, which is a function of the energy dependent complex refractive index and the FZP thickness [11] while in certain cases Δr can have an important impact on the DE (especially for small Δr and large aspect ratio, Ar) [12,13]. Along with the results of the autocorrelation analysis of HXR experiments, the direct imaging results at the SXR range, confirm the functionality of the fabricated ML-FZP for high energies demonstrating the highest resolution imaging ever achieved by a multilayer type Fresnel zone plate

Fabrication of the ML-FZPs
Hard X-ray range experiments
Soft X-ray range experiments
Structure of the multilayer Fresnel zone plate
Focusing hard X-rays
Focusing soft X-rays
Imaging using soft X-rays
Diffraction efficiency at soft X-rays
Findings
Conclusions
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