Abstract
As a type of natural fiber with excellent elongation, coir fiber has been applied in a wide range of fields. To ensure superb performance, coir fiber is usually treated with alkali before being applied. Previous studies paid little attention to the multiple alkali treatment of coir fiber; however, this study focuses on its influence on the mechanical properties of coir fiber and conducts multi-objective optimization and analysis of the tensile strength, elastic modulus and elongation of coir fiber. Our objective is the comprehensive enhancement of the mechanical properties of coir fiber. In this study, the experimental design is based on the Box-Behnken design method, and three treatment parameters were selected for the study, namely NaOH concentration, treatment time and treatment temperature. Analysis of variance (ANOVA) was adopted to analyze the experimental data, and response surface methodology (RSM) was used to investigate how the treatment factors interact with each other and affect the responses values. To improve the tensile strength, elastic modulus and elongation of coir fiber simultaneously, the experimental parameters were optimized. The results showed that the optimal values of NaOH concentration, treatment time and treatment temperature were 4.12%, 15.08 h and 34.21 °C, respectively. Under these conditions, the tensile strength of coir fiber was 97.14 MPa, the elastic modulus was 2.98 GPa and the elongation was 29.35%, which were 38.28%, 39.91% and 25.59% higher than that of untreated coir fiber, respectively. Furthermore, scanning electron microscopy (SEM), thermogravimetric analysis (TGA-DTG), Fourier-transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD) were used to analyze the changes in surface, weight loss, composition and crystallinity of coir fiber treated with alkali under optimum conditions compared with untreated coir fiber to obtain a deeper insight into the influential mechanisms of alkali treatment.
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