Abstract
Both the gas atmosphere (Ar, 15% H2S−H2, H2) and the temperature of treatment strongly affect the distribution of iron atoms among different phases (FeS2-pyrite, Fe1−x S-pyrrhotite, FeS-troilite, mixed Fe−Mo−S structure) in Fe- and FeMo sulfide catalysts. In FeMo sulfide catalysts FeS2 (pyrite) and the Fe−Mo−S structure are stabilized by MoS2.
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