Abstract
Abstract Morphology and structure of starch from fruits of two acorns species, Quercus rotundifolia Lam. (QR) and Quercus suber Lam. (QS), isolated by enzymatic (ENZ) and alkaline (A3S) methods were studied. Acorn starches granules presented a round and oval shape, consisting of medium/small granules, with a mean granule size ranging between 9 and 13 µm. Isolated acorn starches appear as light grayish-brown in naked eye, with high values of L* for starches isolated by the ENZ method, and QR starches were duller than QS. No differences were observed for all the samples in FTIR spectra results. Acorn starches showed a C-type pattern, with a relative crystallinity between 43.1 and 46.6%. The 13C CP/MAS NMR spectra are different for the used isolation methods but are similar for both acorn species. However, acorn-isolated starches presented a predominant A-type allomorph packing type, and the A3S starches showed a higher degree of crystalline material. Those differences in the structure of acorn starches would be helpful to better understand the relationships among structure and functional properties for a possible potential industrial application of chestnut starches.
Highlights
Morphology and structure of starch from fruits of two acorns species, Quercus rotundifolia Lam. (QR) and Quercus suber Lam. (QS), isolated by enzymatic (ENZ) and alkaline (A3S) methods were studied
QR produces starches duller than QS, and the A3S methods presented the higher values. Some of these aspects are probably related to color characteristics of the origin flours since this tendency was observed for QR and QS flours (Correia et al 2009)
Acorn starches showed not to be recommended for use in products requiring light uniform color, but they could find applications in baked goods that are not affected by the starch colour
Summary
Abstract: Morphology and structure of starch from fruits of two acorns species, Quercus rotundifolia Lam. (QR) and Quercus suber Lam. (QS), isolated by enzymatic (ENZ) and alkaline (A3S) methods were studied. Abstract: Morphology and structure of starch from fruits of two acorns species, Quercus rotundifolia Lam. (QS), isolated by enzymatic (ENZ) and alkaline (A3S) methods were studied. Acorn starches showed a C-type pattern, with a relative crystallinity between 43.1 and 46.6%. The 13C CP/MAS NMR spectra are different for the used isolation methods but are similar for both acorn species. Acornisolated starches presented a predominant A-type allomorph packing type, and the A3S starches showed a higher degree of crystalline material. Those differences in the structure of acorn starches would be helpful to better understand the relationships among structure and functional properties for a possible potential industrial application of chestnut starches
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