Abstract
Abstract Depending on the concentration of methanesulfonate in the electrolyte and the hydrodynamic conditions of the process, it is possible to synthesize high-quality films up to 2 mm thickness, free from internal stresses, with reliable adhesion to the substrate in the current density range of 2–180 mA cm−2. The change in the composition of the methanesulfonate electrolyte and the deposition conditions affect the phase composition of lead dioxide. The main difference from oxides obtained from nitrate solutions is the significant α-phase content, which can vary from 17 to 90%. The deposits are polycrystalline and are characterized by smaller crystals. All the results obtained by the X-ray diffraction method are in satisfactory agreement with the scanning electron microscopy data.
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