Abstract
This article presents a morphological, chemical, and fractal dimension study of the time evolution of aluminum AC anodization in 1 M H 3 PO 4 solution. The morphological analysis was accomplished by Atomic Force Microscopy (AFM) and Scanning Electron Microscopy (SEM). According to SEM, ordered porous pattern was already observed after 90 s of anodization, yet AFM revealed a different surface morphology evolution. Stripes were observed on the surface at the initial stages of anodization, developing to the formation of a complete phosphate layer at an intermediate stage and finally, to a porous structure at the steady stage. The phosphate layer was observed by AFM as well as by Auger Electron Spectroscopy (AES). Nevertheless, it could not be noticed by SEM. AFM data were quantified by fractal dimension and no significant changes in terms of fractal dimension were found in the function of the anodization time.
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