Abstract
There are two independent formula units in the asymmetric unit of the title compound, C4H10NO+·C6H2N3O7 −. The morpholinium cations in both molecules are puckered and adopt a chair conformation. Intermolecular N—H⋯O and C—H⋯O interactions generate rings of motifs R 2 1(5) and R 1 2(6). The supramolecular aggregation is completed by the presence of two co-operative hydrogen-bonded networks of further N—H⋯O interactions, which generate an infinite one-dimensional chain along the base vector [100]. Two C—H⋯π interactions are also seen.
Highlights
There are two independent formula units in the asymmetric unit of the title compound, C4H10NO+C6H2N3O7
The supramolecular aggregation is completed by the presence of two co-operative hydrogen-bonded networks of further N—H O interactions, which generate an infinite one-dimensional chain along the base vector [100]
R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger
Summary
Key indicators: single-crystal X-ray study; T = 90 K; mean (C–C) = 0.002 Å; R factor =. 0.029; wR factor = 0.075; data-to-parameter ratio = 9.1. There are two independent formula units in the asymmetric unit of the title compound, C4H10NO+C6H2N3O7. The morpholinium cations in both molecules are puckered and adopt a chair conformation. The supramolecular aggregation is completed by the presence of two co-operative hydrogen-bonded networks of further N—H O interactions, which generate an infinite one-dimensional chain along the base vector [100].
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