Abstract

Abstract The molecular structure of SPF 3 has been determined by gas electron diffraction as follows: r g (PF) = 1.538 ± 0.003 A , r g (SP) = 1.866 ± 0. 005 A and α ) = 99.6 ± 0.3°. The uncertainties represent estimated limits of error. The observed bond lengths and angle for this molecule have been compared with those for related molecules, and empirical equations representing the phosphorus-halogen bond lengths and the valence angles of phosphorus and the other group Vb atoms are obtained.

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