Abstract
The diastereoselective synthesis and structural characterization of a wide range of wholly-synthesis cyclic and acyclic polyacene derivatives has been achieved. These novel compounds are notable for (i) their rigidity, (ii) their highly-ordered structures, and (iii) the high stereochemical precision which governs their formation. A key feature in the success of the synthetic methodology described is the development of a repetitive Diels-Alder reaction sequence in which three distinct levels of diastereoselectivity are expressed during each cycloaddition involving bisdiene and bisdienophilic building blocks
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