Abstract

The aim of this study was to improve the mechanical properties of a slag solidified body at high temperatures. Composite materials with different contents of SiC whiskers were prepared and characterized using techniques such as mechanical testing, scanning electron microscopy (SEM), X-ray diffraction (XRD), thermogravimetric analysis (TGA), and Fourier transform infrared spectroscopy (FT-IR). When the SiC whisker addition is 1% mass percentage, the compressive and tensile strength of the slag solidified body after hydration for 7 days increased by 10.2% and 39.3%, respectively, and Young’s modulus decreased by 16.8%. The results show that the addition of SiC whiskers can enhance the mechanical properties of solidified slag bodies at high temperatures. According to the test results, the hydration products of the slag solidified body mainly consist of honeycomb tobermorite (C-S-H) gel at high temperatures in addition to a small number of spherical products. The spheres are connected to form a dense structure; however, noticeable cracks were present. The addition of SiC whiskers effectively inhibited the initiation and further development of microcracks and improved the bearing capacity of the slag solidified body.

Highlights

  • Well cementing is an important part of drilling and completion engineering [1]

  • The compressive strength of S1 sample is increased by 5.9%, that of S2 is increased by 10.2%, that of S3 is increased by 9.8%, and that of S4 is increased by 10.8%

  • After the SiC whisker is added, these results demonstrate that SiC whiskers can effectively improve the compressive and tensile strength of the slag, improving the overall mechanical properties of the slag solidified body

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Summary

Introduction

Well cementing is an important part of drilling and completion engineering [1]. Improving the displacement efficiency is one of the methods to enhance the quality of cementing in complex oil and gas wells [2]. In the investigation of cementitious materials with similar hydraulic properties to cement, blast furnace slag, with its high activity, high early strength, and low cost, has received considerable attention [4]. Slag mud-tocement (MTC) technology was originally developed with slag as the cementing material. Is refers to the process where the blast furnace water quench slag is replaced by traditional weighted materials and is mixed into the drilling fluid, such that the drilling fluid itself or the drilling fluid filter cake contains potentially active slag [7]. Specific activators are added during the drilling and completion process to ensure that the drilling fluid contains slag and that the drilling fluid filter cake has curing abilities when cementing [8]. The chloride ion diffusion coefficient and water absorption rate of alkali-activated slag

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