Abstract

Concept, design and practical implementation of a miniaturized spectrophotometer, utilized as a mid-infrared-based multi gas sensor is described. The sensor covers an infrared absorption wavelength range of 2.9 to 4.8 um, providing detection capabilities for carbon dioxide, carbon monoxide, nitrous oxide, sulphur dioxide, ammonia and methane. A lead selenide photo-detector array and customized MEMS-based micro-hotplate are used as the detector and broadband infrared source, respectively. The spectrophotometer optics are based on an injection moulded Schwarzschild configuration incorporating optical pass band filters for the spectral discrimination. This work explores the effects of using both fixed-line pass band and linear variable optical filters. We report the effectiveness of this low-power-consumption miniaturized spectrophotometer as a stand-alone single and multi-gas sensor, usage of a distinct reference channel during gas measurements, development of ideal optical filters and spectral control of the source and detector. Results also demonstrate the use of short-time pulsed inputs as an effective and efficient way of operating the sensor in a low-power-consumption mode. We describe performance of the spectrometer as a multi-gas sensor, optimizing individual component performances, power consumption, temperature sensitivity and gas properties using modelling and customized experimental procedures.

Highlights

  • Non-dispersive infrared (NDIR) sensors are emerging as a replacement for chemical-based gas sensors [9,10,11,12,13], addressing inherent problems with chemical sensors such as short lifespan due to gradual degradation of the catalyst, high power consumption, susceptibility to gas poisoning and consequent non-fail to safe [9]

  • The NDIR-based gas sensor described in this work addresses these shortfalls

  • NDIR sensors are based on different gases absorbing infrared radiation at uniquely defined wavelengths [22]

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Summary

Introduction

Non-dispersive infrared (NDIR) sensors are based on mid-infrared absorption spectroscopy [1,2], providing benefits such as cost and sensitivity [1,2,3,4], integration as a miniaturised sensor configuration compared to other optical-based gas-sensing techniques [5] such as tunable diode laser absorption spectroscopy [6], photoacoustic spectroscopy [7] and quartz-enhanced photoacoustic spectroscopy [8].NDIR sensors are emerging as a replacement for chemical-based gas sensors [9,10,11,12,13], addressing inherent problems with chemical sensors such as short lifespan due to gradual degradation of the catalyst, high power consumption, susceptibility to gas poisoning and consequent non-fail to safe [9]. Non-dispersive infrared (NDIR) sensors are based on mid-infrared absorption spectroscopy [1,2], providing benefits such as cost and sensitivity [1,2,3,4], integration as a miniaturised sensor configuration compared to other optical-based gas-sensing techniques [5] such as tunable diode laser absorption spectroscopy [6], photoacoustic spectroscopy [7] and quartz-enhanced photoacoustic spectroscopy [8]. The NDIR-based gas sensor described in this work addresses these shortfalls. NDIR sensors are based on different gases absorbing infrared radiation at uniquely defined wavelengths [22]. When compared with available electrolytic gas detectors, NDIR sensors can provide enhanced accuracy, operate at lower power, are not Sensors 2020, 20, 3843; doi:10.3390/s20143843 www.mdpi.com/journal/sensors

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