Abstract
A new co-crystal complex [Ni7(emmp)6(CH3O)2(OH)4][Ni(emmp)2]·(ClO4)2 (1, Hemmp is 2-ethoxy-6-methyliminomethyl-phenol) has been synthesised by microwave-assisted method. Complex 1 was characterised by IR spectroscopy, elemental analysis, Raman spectroscopy and X-ray single-crystal diffraction. The complex consists of a heptanuclear cation cluster [Ni7(emmp)6(CH3O)2(OH)4]2+, a mononuclear complex [Ni(emmp)2] and two counteranions. Complex 1 displays the contents of antiferromagnetic and ferromagnetic properties.
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