Abstract
Single crystalline Co 3O 4 nanorods have been successfully synthesized through thermal decomposition of the precursor, which was obtained by the microwave-assisted hydrothermal route. The obtained sample was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared spectrometer (FT-IR), and X-ray photoelectron spectroscopy (XPS). The results confirm that the resulting oxide was pure single-crystalline Co 3O 4 nanorods. The optical property test indicates that the absorption peak of the nanorods shifts towards short wavelength. And the blue shift phenomenon might be ascribed to the quantum effect.
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