Abstract

New synthesis method of hydrotalcites using microwave irradiation is presented, which avoids the autoclave high temperature treatment as well as the long crystallization time. The crystallite size of the obtained solids is smaller than in the conventionally prepared hydrotalcites. The highest irradiation time provided the lowest aluminium incorporation to the hydrotalcite network. Diminishing microwave irradiation time produces purer hydrotalcites. If the gel is irradiated only for two minutes a well crystallized hydrotalcite is obtained.

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