Microwave hydrothermal synthesis and visible-light photocatalytic activity of γ-Bi 2MoO 6 nanoplates

Abstract

γ-Bi 2MoO 6 nanoplates have been successfully synthesized by a microwave hydrothermal approach for the first time, by using Bi(NO 3) 3, NH 3 and MoO 3 as the starting materials. The influences of the various preparation parameters (including the pH value, reaction temperature, and holding time) on the phase formation and morphology development were investigated in detail. XRD and TEM results showed that γ-Bi 2MoO 6 nanocrystals were formed indirectly with an intermediate phase of Bi 2O 3 in the microwave hydrothermal and hydrothermal synthesis. However, the reaction condition in the microwave hydrothermal approach was milder compared with the hydrothermal method. The photocatalytic activity of the nanoplates was evaluated by the degradation of the methylene blue solution under visible-light irradiation.