Abstract
Anhydrous basic bismuth nitrate Bi6(NO3)2O7(OH)2 was shown to be produced by reacting bismuth nitrate with aqueous ammonia under microwave-assisted hydrothermal treatment as a result of hydrolysis. The composition of the basic nitrate was verified by titration, CHNS analyses, DTG, and IR spectroscopy. Photocatalytic tests showed that Bi6(NO3)2O7(OH)2 has a photocatalytic activity, but its properties are interior to those of α-Bi2O3.
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