Microtensile testing of dentin adhesives

Abstract

Objectives. This study was conducted in order to compare the microtensile and shear bond strengths of five commercial dentin adhesive systems. Scotchbond Multipurpose with maleic acid (SM), Scotchbond Multipurpose with phosphoric acid (SP), Scotchbond Multipurpose Plus (SBP), Clearfil Liner Bond System (CL), and Prime and Bond (PB) were tested. Methods. Thirty extracted unerupted third molars, in groups of six teeth per adhesive system, were prepared for microtensile testing. The specimens were tested following a 24 h incubation at 37°C in normal saline. Shear bond testing was performed on 35 additional teeth, using seven teeth per adhesive system. After testing, the fracture sites were observed using light microscopy and a scanning electron microscope to determine the type of failure involved. Results. The microtensile test results (mean±SD) were SM, 24.6±7.2 MPa; SP, 28.8±11.8 MPa; SBP, 22.7±6.5 MPa; PB, 25.5±9.4 MPa; and CL, 36.8±10.0 MPa. A Bonferroni post-hoc test showed significantly ( p<0.05) greater strength for CL compared to SM, SP, SBP, and PB. The shear bond strength test results were SM, 19.4±4.4 MPa; SP, 24.5±8.4 MPa; SBP, 15.3±4.9 MPa; PB, 23.2±7.1 MPa; and CL, 24.8±3.5 MPa. No statistically significant differences were found among the shear bond strength test results. The shear bond test produced significantly more failures within dentin and composite than the microtensile method. Significance. It is concluded that the microtensile test produced a more definitive assessment of adhesive bond strength than the shear bond test. Microtensile testing showed CL to be significantly stronger than SM, SP, SBP, and PB ( p<0.05).