Abstract
Conversion films of vanadium oxides are potentiodynamically generated on vanadium in acetate electrolyte systems at high voltages. The microstructure of the about 5 μm thin anodic films is investigated. X-ray diffraction and transmission electron microscopy indicate the films are complete amorphous. X-ray photoelectron spectroscopy (XPS) measurements show V 2p 3/2 binding energies of mixed valance vanadium sub oxides. Electron spin resonance (ESR) experiments on isolated films at 130 K point to paramagnetic V 4+ centers in a disordered octahedral oxygen surrounding.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
